5-Methylfurfural → HCID 66723148, compound

HRID 505706Notes

Reaction equation

HRID 505706 reaction equation
[CH3:1][O:2][C:3]([C:5]1[CH:14]=[CH:13][C:12]2[C:11](=[O:15])[CH2:10][CH2:9][CH2:8][C:7]=2[CH:6]=1)=[O:4].[CH3:16][C:17]1[O:21][C:20]([CH:22]=O)=[CH:19][CH:18]=1>>[CH3:22][C:20]1[O:21][C:17]([CH:16]=[C:10]2[CH2:9][CH2:8][C:7]3[CH:6]=[C:5]([C:3]([O:2][CH3:1])=[O:4])[CH:14]=[CH:13][C:12]=3[C:11]2=[O:15])=[CH:18][CH:19]=1

Participants

3

Reactant 2

HCID 120975-MethylfurfuralHCID 15309116Methyl 5-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate

Product 1

HCID 66723148HCID 66723148, compound

Procedure

The title compound was prepared according to Method A3 from 5-oxo-5,6,7,8-tetrahydronaphtalene-2-carboxylic acid methyl ester (396 mg, 1.9 mmol) and 5-methyl-2-furaldehyde (192 mg, 2.0 mmol). ES-MS m/z 297 (M+H).

Sources & evidence

ORD record
ord-b3c3230f1f35477da9d7fc6ce576fffc
Source dataset
uspto-grants-2010_08
Patent number
US07781428B2

Reaction notes

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