HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanemethanol → HCID 68799259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanemethanol | HCID 7507 | — |
| Reactant | (+/-)(3SR,3aRS)-2-(3-chloro-4-cyanophenyl)-3-cyclopentyl-3,3a,4,5-tetrahydro-2H-benzo[g]indazole-7-carboxylic acid | HCID 24983760 | — |
| Product | HCID 68799259 | HCID 68799259 | 67% |
Reaction Steps
The title compound was prepared from (±)-(3SR,3aRS)-2-(3-chloro-4-cyanophenyl)-3-cyclopentyl-3,3a,4,5-tetrahydro-2H-benzo[g]indazole-7-carboxylic acid, Example 15 and cyclohexylmethanol according to Method E (yellow solid, 165 mg, 0.320 mmol, 67% yield). ES-HRMS m/z calc. for C31H35ClN3O2 (M+H) 516.2412, found 516.2403.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781428B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-620e278348674e6a9baa9411dadb4e87 |
| Source note | uspto-grants-2010_08 |