HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-(2-Hydroxyethyl)pyridine → (+/-)-(3SR,3aRS)-2-(pyridin-2-yl)ethyl 2-(3-chloro-4-cyanophenyl)-3-cyclopentyl-3,3a,4,5-tetrahydro-2H-benzo[g]indazole-7-carboxylate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-(2-Hydroxyethyl)pyridine | HCID 7675 | — |
| Edukt | (+/-)(3SR,3aRS)-2-(3-chloro-4-cyanophenyl)-3-cyclopentyl-3,3a,4,5-tetrahydro-2H-benzo[g]indazole-7-carboxylic acid | HCID 24983760 | — |
| Produkt | (+/-)-(3SR,3aRS)-2-(pyridin-2-yl)ethyl 2-(3-chloro-4-cyanophenyl)-3-cyclopentyl-3,3a,4,5-tetrahydro-2H-benzo[g]indazole-7-carboxylate | HCID 68802418 | — |
Reaktionsschritte
The title compound was prepared according to Method E from (±)-(3SR,3aRS)-2-(3-chloro-4-cyanophenyl)-3-cyclopentyl-3,3a,4,5-tetrahydro-2H-benzo[g]indazole-7-carboxylic acid, Example 15 and 2-(2-pyridyl)ethanol. Yellow solid, 194 mg. ES-MS m/z 525 (M+H).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07781428B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-58c97a9408444b5093467641d724b9de |
| Quellennotiz | uspto-grants-2010_08 |