huagongshe.com
HRID505812

反应详情

EQUATION

反应方程式

HRID 505812 的结构方程式

REACTANTS

反应物

1
结构：COC(=O)c1cc2c(s1)c(C1CCCCC1)c(-c1ccc(Cl)cc1)n2CC(=O)OC(C)(C)C
HCID68467870

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C1C=C2C(=C(C3CCCCC3)C(c3ccccc3)(c3ccc(Cl)cc3)N2CC(=O)O)S1
HCID68470301

未命名化合物

收率 94%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl.O=C(O)C(F)(F)F
溶剂HCID21863450

未命名化合物

PROCEDURE

实验过程

A solution (0.04 M) of methyl 4-(2-tert-butoxy-2-oxoethyl)-6-cyclohexyl-5-(4-chlorophenyl)-4H-thieno[3,2-b]pyrrole-2-carboxylate in DCM/TFA (1:1) was stirred at RT for 3 h. Evaporation of the solvent gave the title compound (94%) as a solid.

WORKUP

后处理

  1. customEvaporation of the solvent