Cyclohexanamine, 3,3,5-trimethyl- → HCID 68465716, compound

HRID 505957Notes

Reaction equation

HRID 505957 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([S:9]([N:12]=[CH:13][N:14]([CH3:16])[CH3:15])(=[O:11])=[O:10])=[CH:5][C:4]=1[CH2:17]Cl.[CH3:19][C:20]1([CH3:28])[CH2:25][CH:24]([CH3:26])[CH2:23][CH:22]([NH2:27])[CH2:21]1>C(Cl)Cl>[CH3:15][N:14]([CH:13]=[N:12][S:9]([C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[C:4]([CH2:17][NH:27][CH:22]2[CH2:23][CH:24]([CH3:26])[CH2:25][C:20]([CH3:28])([CH3:19])[CH2:21]2)[CH:5]=1)(=[O:11])=[O:10])[CH3:16]

Participants

4

Reactant 2

HCID 85931Cyclohexanamine, 3,3,5-trimethyl-HCID 68464912HCID 68464912, compound

Product 1

HCID 68465716HCID 68465716, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of 0.2 g of 4-methoxy-3-chloromethyl-N-dimethylaminomethylenephenylsulfon-amide, 0.37 ml of 3,3,5-trimethylcyclohexylamine and 5 ml of methylene chloride is stirred at RT for 24 hours and then concentrated in vacuo.

Workup

  1. concentrationconcentrated in vacuo

Sources & evidence

ORD record
ord-dac0c1be16ff483bbdf0400c8f06831d
Source dataset
uspto-grants-2010_08
Patent number
US07781613B2

Reaction notes

Loading…