HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 50616Generated: October 31, 2026
Water → N-isopropyl-6-nitro-1,2,3,4-tetrahydrocarbazole
https://huagongshe.com/reaction/50616
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Isopropyl iodide | HCID 6362 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 6-nitro-2,3,4,9-tetrahydro-1H-carbazole | HCID 258747 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-isopropyl-6-nitro-1,2,3,4-tetrahydrocarbazole | HCID 22736139 | 43.2% |
Reaction Steps
6-Nitro-1,2,3,4-tetrahydrocarbazole (5.04 g) prepared by the method described in Journal of Chemical Society, p.833 (1924) was dissolved in 50 mL of acetone, and the solution was added with 2.25 g of potassium hydroxide and 8.45 g of isopropyl iodide, warmed to 50° C., and stirred for 3 hours. Water was added to the reaction mixture, and the deposited precipitates were collected to obtain 2.60 g of N-isopropyl-6-nitro-1,2,3,4-tetrahydrocarbazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06713473B1 |
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| Source dataset | uspto-grants-2004_03 |
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| ORD ID | ord-310fd1766b4945f4a8e7fd852853b56d |
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| Source note | uspto-grants-2004_03 |
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