HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 67061224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 1,2-BIS(2-MEO-ETO)BENZENE | HCID 3304577 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67061224 | HCID 67061224 | 99.6% |
Reaction Steps
1,2-Bis(2-methoxyethoxy)benzene (8.1 g, 31.9 mmol) and N-bromosuccinimide (6.2 g, 35 mmol) were stirred in 50 mL DMF at room temperature overnight. The reaction was diluted with 200 mL EtOAc and washed with 1N NaOH and water. The organic layer was dried over magnesium sulfate and concentrated to give 9.7 g (92%) of 4-bromo-1,2-bis(2-methoxyethoxy)benzene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07781591B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-6055e416fc634130b6a5999500db282f |
| Source note | uspto-grants-2010_08 |