HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Methylimidazole → 2-(2-Methyl-1H-imidazol-1-yl)ethan-1-amine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Methylimidazole | HCID 12749 | — |
| Edukt | 2-Chloroethylamine hydrochloride | HCID 9793737 | — |
| Produkt | 2-(2-Methyl-1H-imidazol-1-yl)ethan-1-amine | HCID 3157480 | 47% |
Reaktionsschritte
2-(2-Methylimidazol-1-yl)ethylamine was prepared from 2-methylimidazole and 2-chloroethylamine hydrochloride using the method described in Step B of Example 1. This material was obtained as a light yellow oil in 47% yield. 1H NMR (300 MHz, CD3OD) δ 6.95 (br s, 1H), 6.82 (br s, 1H), 4.90 (bs, 2H), 3.90 (t, J=6.9 Hz, 2H), 2.93 (t, J=6.9 Hz, 2H), 2.35 (s, 3H); MS (APCI) m/z 126 [M+H]+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07781430B2 |
| Quelldatensatz | uspto-grants-2010_08 |
| ORD ID | ord-ef143cb139f24853b6983daf34d09806 |
| Quellennotiz | uspto-grants-2010_08 |