Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N-(3-ethynylphenyl)acetamide → HCID 11530439, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N-(3-ethynylphenyl)acetamide | HCID 2726447 | — |
| 반응물 | Potassium tert-butoxide | HCID 23665647 | — |
| 반응물 | N-[3-(5-Nitro-1H-pyrrolo[2,3-b]pyridin-2-yl)phenyl]acetamide | HCID 68462732 | — |
| 생성물 | HCID 11530439 | HCID 11530439 | — |
반응 단계
Was prepared analogously to example 9-2 starting from 3-(acetylamino)phenylacetylene. In the preparation of the intermediate N-[3-(5-nitro-1H-pyrrolo[2,3-b]pyridin-2-yl)-phenyl]-acetamide by cyclization reaction an higher equimolar amount of base (Potassium tert-butoxide) as in Example 2-2 is needed:
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07786113B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-0774e8029cfd452db3d7f46a1be6b461 |
| 출처 메모 | uspto-grants-2010_08 |