HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 16679026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | HCID 16679702 | HCID 16679702 | — |
| Product | HCID 16679026 | HCID 16679026 | 15% |
Reaction Steps
The title compound was synthesized in analogy to example 17, from 9-(3-pyrrolidin-1-yl-propoxy)-2,3,4,5-tetrahydro-[1,4]diazepino[1,2-a]indol-1-one (example 16), 2-bromoethyl methyl ether and sodium hydride, to give the desired product as a colorless oil (15%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786109B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-7650912fe3054078a1d9c6b8db4069e9 |
| Source note | uspto-grants-2010_08 |