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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 506755Generated: November 2, 2026

HCID 68424210, compound → HCID 86612932, compound

https://huagongshe.com/reaction/506755

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68424210HCID 68424210—
CatalystHCID 178418406HCID 178418406—
SolventDichloromethaneHCID 6344—
ProductHCID 86612932HCID 8661293274%

Reaction Steps

The suspension of 0.3 g (1.2 mmol) (5-benzyloxy-1H-pyrrolo[2,3-b]pyridin-2-yl)-methanol and 0.82 g (9.4 mmol) manganese dioxide in 15 ml dichloromethane was stirred 3 h at room temperature. After filtration over Dicalite Speed Plus® (Aldrich) the solvent was evaporated to give 0.22 g (74%) of the desired compound as a light brown solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07786109B2
Source datasetuspto-grants-2010_08
ORD IDord-5a2316016eda4fbd9140eeecafc462c8
Source noteuspto-grants-2010_08