HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 68469577, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 68467757 | HCID 68467757 | — |
| Product | HCID 68469577 | HCID 68469577 | 32% |
Reaction Steps
The product is prepared by following the procedure described in example 34 stage (k), starting with 0.050 g of [2-(5,6-dimethoxy-1-methyl-1H-pyrrolo[3,2-b]pyridin-3-yl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-ylmethyl]-(3-piperidin-1-yl-propyl)amine instead of the cyclopropyl-[2-(5,6-dimethoxy-1-methyl-1H-pyrrolo[3,2-b]pyridin-3-yl)-1-(toluene-4-sulfonyl)-1H-pyrrolo[2,3-b]pyridin-4-ylmethyl]amine used in example 34 stage (k) and 0.324 cm3 of 5N potassium hydroxide. 0.012 g of [2-(5,6-dimethoxy-1-methyl-1H-pyrrolo[3,2-b]pyridin-3-yl)-1H-pyrrolo[2,3-b]pyridin-4-ylmethyl]-(3-piperidin-1-yl-propyl)amine is obtained with the following characteristics:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786114B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-601c9865ea9b44f29f16635c60bd3c2b |
| Source note | uspto-grants-2010_08 |