HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 72569089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 68639007 | HCID 68639007 | — |
| Reactant | HCID 72569092 | HCID 72569092 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 72569089 | HCID 72569089 | 19% |
Reaction Steps
300 mg (0.33 mmol) of product 11 and 0.8 ml of diethylamine are solved in 4 ml DMF (dimethylformamide) and reacted according to production of compound 9. 42 mg (19%) of compound 12 is obtained in form of an amorphic solid compound: C39H43N7O5 (689.82) MS (ESI+) 690.3 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786103B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-46813c8a90a549e284d91ca377a75fe5 |
| Source note | uspto-grants-2010_08 |