HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 68467367, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Stannous Chloride | HCID 24479 | — |
| Reactant | HCID 68463081 | HCID 68463081 | — |
| Product | HCID 68467367 | HCID 68467367 | — |
Reaction Steps
2 g of 4-[tert-butoxycarbonyl-(4-trifluoromethoxy-benzyl)-amino]-3-nitro-benzoic acid allyl ester (4.0 mmol) were dissolved in 20 ml DMF. 2.8 g SnCl2×2 H2O (12 mmol) are added and the reaction stirred at room temperature for 16 h. The crude was filtered over Kieselgel and the solvent evaporated. MS(ISP): 467.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786128B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-8ffd37855aec46bf889ddd38a8ee3b83 |
| Source note | uspto-grants-2010_08 |