HCID 21015128, compound → HCID 21015133, compound

HRID 507432Notes

Reaction equation

C[O:2][C:3]([CH:5]1[CH2:9][S:8][CH:7]2[CH2:10][CH:11]([NH:14][C:15]([O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[O:16])[C:12](=[O:13])[N:6]12)=O.[NH3:22].CO>>[C:18]([O:17][C:15](=[O:16])[NH:14][CH:11]1[C:12](=[O:13])[N:6]2[CH:7]([S:8][CH2:9][CH:5]2[C:3](=[O:2])[NH2:22])[CH2:10]1)([CH3:21])([CH3:20])[CH3:19]

Participants

Reactant 2

HCID 21015128HCID 21015128, compound

HCID 21705897Ammonia methanol

Product 1

HCID 21015133HCID 21015133, compound

Procedure

Compound 4 (0.5 g, 1.58 mmol) was treated with NH3/MeOH (20 mL) at room temperature and stirred overnight. The crude product was obtained by evaporation and used directly in the next step.

Sources & evidence

ORD record: ord-c4e7d64c42404347a052959598f76aea
Source dataset: uspto-grants-2010_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07786163B2

Reaction notes

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