HRID507511

反应详情

EQUATION

反应方程式

HRID 507511 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of tert-butyl 2-(2-nitrophenylamino)ethylcarbamate (400 mg) and palladium (10% on activated carbon, 20 mg) in ethanol (50 mL) was stirred under hydrogen (1 atm) for 5 h. The mixture was filtered through Celite and washed with methanol. The solvent was removed and the product was used in the next step without further purification.

WORKUP

后处理

  1. filtrationThe mixture was filtered through Celite
  2. washwashed with methanol
  3. customThe solvent was removed
  4. customthe product was used in the next step without further purification