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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 507718Generated: November 3, 2026

Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)

https://huagongshe.com/reaction/507718

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzobisisobutyronitrileHCID 6547—
ReactantStyreneHCID 7501—
ReactantAcrylonitrileHCID 7855—
ReactantTricalcium PhosphateHCID 24456—
SolventWaterHCID 962—
ProductProp-2-enenitrile--ethenylbenzene (1/1)HCID 62696—

Reaction Steps

72 parts of styrene, 28 parts of acrylonitrile, 120 parts of deionized water and 0.2 parts of azobisisobutylonitrile (AIBN) are mixed. To the mixture, 0.4 parts of tricalciumphosphate and 0.2 parts of mercaptan-containing chain transfer agent are added. The resultant solution is heated to 80° C. for 90 minutes and kept for 240 minutes. The resultant product is washed, dehydrated and dried to obtain styrene-acrylonitrile copolymer resin (SAN) in powder form. The weight average molecular weight of the styrene-acrylonitrile copolymer resin is 180,000 to 200,000.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07786196B2
Source datasetuspto-grants-2010_08
ORD IDord-680c2c775cba4a429e4d1cbf9ee29201
Source noteuspto-grants-2010_08