Thionyl Chloride → HCID 123203838, compound

Participants

Reaction Steps

4-diisopropylsilanyl benzoic acid (1) (6.7 g, 28.4 mmol) and thionyl chloride (3.2 mL, 42.6 mmol) were mixed together and heated to reflux for 2 hours. a desired compound was then purified and identified by distillation under a reduced pressure (1 mmHg, 102-104° C.) (5.6 g, 77%). Its NMR data are as follows:

Provenance & Evidence