HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86601709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | HCID 68470768 | HCID 68470768 | — |
| Reactant | HCID 68471405 | HCID 68471405 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 86601709 | HCID 86601709 | 100.3% |
Reaction Steps
26.2 g of 4-(8-(4-chalconyloxy)octanoxy)phenylmaleimide, 22.7 g of 4-(8-(4-chalconyloxy)octanoxy)styrene and 3.0 g of azobisisobutyronitrile were dissolved in 500 ml of dimethyl acetamide to carry out a reaction in a nitrogen atmosphere at 80° C. for 10 hours. A viscous reaction mixture was added to methanol to precipitate a polymer which was then dried to obtain 49 g of a 4-(8-(4-chalconyloxy)octanoxy)phenylmaleimide/4-(8-(4-chalconyloxy)octanoxy)styrene alternating copolymer. This polymer was designated as polymer “c”.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07787085B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-78d3641761014d9a945ba3edb9bfe050 |
| Source note | uspto-grants-2010_08 |