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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 507903Generated: November 3, 2026

Methanol → HCID 86601709, compound

https://huagongshe.com/reaction/507903

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantAzobisisobutyronitrileHCID 6547—
ReactantHCID 68470768HCID 68470768—
ReactantHCID 68471405HCID 68471405—
SolventDimethylacetamideHCID 31374—
ProductHCID 86601709HCID 86601709100.3%

Reaction Steps

26.2 g of 4-(8-(4-chalconyloxy)octanoxy)phenylmaleimide, 22.7 g of 4-(8-(4-chalconyloxy)octanoxy)styrene and 3.0 g of azobisisobutyronitrile were dissolved in 500 ml of dimethyl acetamide to carry out a reaction in a nitrogen atmosphere at 80° C. for 10 hours. A viscous reaction mixture was added to methanol to precipitate a polymer which was then dried to obtain 49 g of a 4-(8-(4-chalconyloxy)octanoxy)phenylmaleimide/4-(8-(4-chalconyloxy)octanoxy)styrene alternating copolymer. This polymer was designated as polymer “c”.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07787085B2
Source datasetuspto-grants-2010_08
ORD IDord-78d3641761014d9a945ba3edb9bfe050
Source noteuspto-grants-2010_08