HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → HCID 178519697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 4-Aminobenzyl alcohol | HCID 69331 | — |
| Reactant | 4-Phenyl-1,3-thiazole-2-carbaldehyde | HCID 3538814 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 178519697 | HCID 178519697 | 88.3% |
Reaction Steps
A mixture of 4-phenyl-1,3-thiazole-2-carbaldehyde (1.10 g, 5.81 mmol), (4-aminophenyl)methanol (615 mg, 5.0 mmol), acetic acid (0.4 mL) and 1,2-dichloroethane (10 mL) was stirred at room temperature for 30 min. The reaction mixture was diluted with hexane. The precipitated solid was collected by filtration, washed with hexane, and dried to give the title compound (1.30 g, yield 88%) as yellow crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07786165B2 |
| Source dataset | uspto-grants-2010_08 |
| ORD ID | ord-c030fbe8d23e465e8c1700c584484805 |
| Source note | uspto-grants-2010_08 |