HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → 4-(Bromomethyl)-2-chloro-1-methoxybenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | 3-Chloro-4-methoxytoluene | HCID 140873 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 4-(Bromomethyl)-2-chloro-1-methoxybenzene | HCID 11470370 | — |
Reaction Steps
To a solution of 2-chloro-1-methoxy-4-methylbenzene (300 mg, 1.92 mmol) in carbon tetrachloride (10.0 mL) was added N-bromosuccinimide (445 mg, 2.50 mmol) and benzoylperoxide (4.6 mg, 0.0192 mmol) and the reaction heated to reflux for 4.5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096500B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d704e55e5af34d059120aabbf7e922fa |
| Source note | uspto-grants-2015_08 |