化工社化工社 化学情報印刷レポート · 研究参考用
Oxalyl chloride → 2-Fluoro-4-(trifluoromethyl)benzoyl isocyanate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | 2-Fluoro-4-(trifluoromethyl)benzamide | HCID 605689 | — |
| 溶媒 | 1,2-Dichloroethane | HCID 11 | — |
| 生成物 | 2-Fluoro-4-(trifluoromethyl)benzoyl isocyanate | HCID 90019717 | — |
反応手順
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 2-fluoro-4-(trifluoromethyl)benzamide (0.200 g, 0.96 mmol), EDC (10 mL) and oxalyl chloride (0.1 mL, 1.15 mmol) to afford 0.200 g of the product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09096545B2 |
| 出典データセット | uspto-grants-2015_08 |
| ORD ID | ord-33caabd6fd8a4d2b825ad1a16d0ef143 |
| 出典メモ | uspto-grants-2015_08 |