Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Oxalyl chloride → 4-Trifluoromethylbenzoylisocyanate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 반응물 | 4-(Trifluoromethyl)benzamide | HCID 74684 | — |
| 용매 | 1,2-Dichloroethane | HCID 11 | — |
| 생성물 | 4-Trifluoromethylbenzoylisocyanate | HCID 14913744 | — |
반응 단계
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 4-(trifluoromethyl)benzamide (0.200 g, 1.05 mmol), EDC (10 mL) and oxalyl chloride (0.15 mL, 1.58 mmol) to afford 0.200 g of the product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09096545B2 |
| 출처 데이터셋 | uspto-grants-2015_08 |
| ORD ID | ord-5a698731a634490a97a01e743c879920 |
| 출처 메모 | uspto-grants-2015_08 |