HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalyl chloride → 3-((2,2,2-Trifluoroacetamido)methyl)-2,6-dimethylbenzoyl isocyanate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Edukt | 3-((2,2,2-Trifluoroacetamido)methyl)-2,6-dimethylbenzamide | HCID 90019133 | — |
| Lösungsmittel | 1,2-Dichloroethane | HCID 11 | — |
| Produkt | 3-((2,2,2-Trifluoroacetamido)methyl)-2,6-dimethylbenzoyl isocyanate | HCID 90019298 | — |
Reaktionsschritte
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 3-((2,2,2-trifluoroacetamido)methyl)-2,6-dimethylbenzamide (1.0 g, 3.6 mmol), oxalyl chloride and EDC (10 mL) to afford 0.900 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09096545B2 |
| Quelldatensatz | uspto-grants-2015_08 |
| ORD ID | ord-393dacc85e7b4419aa087ca78a46b698 |
| Quellennotiz | uspto-grants-2015_08 |