HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Oxalyl chloride → 4-Fluoro-3-(trifluoromethyl)benzoyl isocyanate
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Oxalyl chloride | HCID 65578 | — |
| Edukt | 4-Fluoro-3-(trifluoromethyl)benzamide | HCID 144254 | — |
| Lösungsmittel | 1,2-Dichloroethane | HCID 11 | — |
| Produkt | 4-Fluoro-3-(trifluoromethyl)benzoyl isocyanate | HCID 90019295 | — |
Reaktionsschritte
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 4-fluoro-3-(trifluoromethyl)benzamide (0.200 g), oxalyl chloride (0.012 mL) and EDC (15 mL) to afford 0.150 g of the desired product.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09096545B2 |
| Quelldatensatz | uspto-grants-2015_08 |
| ORD ID | ord-0cb36496f4d44dc682c84e6783475d65 |
| Quellennotiz | uspto-grants-2015_08 |