化工社化工社 化学情報印刷レポート · 研究参考用
1-Chloro-3-ethynyl-2-fluorobenzene → 1-(4-((3-Chloro-2-fluorophenyl)ethynyl)-3-methoxyphenyl)-3-(2-chloro-6-fluorophenyl)-1H-1,2,4-triazol-5(4H)-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Chloro-3-ethynyl-2-fluorobenzene | HCID 63033487 | — |
| 反応物 | 3-(2-chloro-6-fluorophenyl)-1-(4-iodo-3-methoxyphenyl)-1H-1,2,4-triazol-5(4H)-one | HCID 136492497 | — |
| 生成物 | 1-(4-((3-Chloro-2-fluorophenyl)ethynyl)-3-methoxyphenyl)-3-(2-chloro-6-fluorophenyl)-1H-1,2,4-triazol-5(4H)-one | HCID 136612569 | — |
反応手順
The title compound was prepared according to the procedure described in Example-3 using 3-(2-chloro-6-fluorophenyl)-1-(4-iodo-3-methoxyphenyl)-1H-1,2,4-triazol-5(4H)-one (Intermediate-32, 0.050 g, 0.11 mmol), 1-chloro-3-ethynyl-2-fluorobenzene
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09096545B2 |
| 出典データセット | uspto-grants-2015_08 |
| ORD ID | ord-6299eb6ff84a4d64bad6fca8ed87f0bf |
| 出典メモ | uspto-grants-2015_08 |