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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 509727Generated: October 28, 2026

2-Methyl-5-vinylpyridine → HCID 57876205, compound

https://huagongshe.com/reaction/509727

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Methyl-5-vinylpyridineHCID 8817—
ReactantPotassium HydroxideHCID 14797—
ReactantHCID 68759840HCID 68759840—
SolventN-methyl-2-pyrrolidoneHCID 13387—
ProductHCID 57876205HCID 57876205—

Reaction Steps

The title compound is prepared from a mixture of 4-(3,4-dihydro-8-methyl-1H-pyrido[4,3-b]indol-2(5H)-yl)benzenamine, 2-methyl-5-vinylpyridine and KOH (5-7 equiv) in NMP at a temperature ranging between 25 deg C. to 100 deg C. The product obtained is isolated by preparative HPLC.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09096591B2
Source datasetuspto-grants-2015_08
ORD IDord-402b125cf7434ab4849aac7934450e63
Source noteuspto-grants-2015_08