Diiodomethane → HCID 86720053, compound

Participants

Reaction Conditions

Reaction Steps

To a mixture of 2.59 ml (32.20 mmol) of diiodomethane and 2.78 ml (20.61 mmol) of isoamyl nitrite were added 539 mg (approx. 1.08 mmol) of the compound from example 115, and the reaction mixture was stirred at 85° C. overnight. The mixture was concentrated, and the residue was stirred with dichloromethane and filtered. The solids were washed with dichloromethane and dried under high vacuum. 330 mg of the title compound were obtained (92% purity; 53% of theory).

Provenance & Evidence