Azetidine → HCID 59612876, compound

HRID 510479Notes

Reaction equation

HRID 510479 reaction equation
Cl[C:2]1[N:7]=[C:6]([CH3:8])[C:5]([N+:9]([O-:11])=[O:10])=[CH:4][CH:3]=1.[NH:12]1[CH2:15][CH2:14][CH2:13]1>>[N:12]1([C:2]2[N:7]=[C:6]([CH3:8])[C:5]([N+:9]([O-:11])=[O:10])=[CH:4][CH:3]=2)[CH2:15][CH2:14][CH2:13]1

Participants

3

Reactant 2

HCID 10422AzetidineHCID 2531236-Chloro-2-methyl-3-nitropyridine

Product 1

HCID 59612876HCID 59612876, compound

Procedure

Prepared from 6-chloro-2-methyl-3-nitropyridine and azetidine following the method used to prepare Intermediate 46. LCMS (ES+) 194 (M+H)+, RT 2.55 minutes (method 1).

Workup

  1. customLCMS (ES+) 194 (M+H)+, RT 2.55 minutes (method 1)

Sources & evidence

ORD record
ord-19c440045a154020a43d2035830620c8
Source dataset
uspto-grants-2015_08
Patent number
US09096614B2

Reaction notes

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