HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 57467210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57467212 | HCID 57467212 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57467210 | HCID 57467210 | — |
Reaction Steps
tert-Butyl [1-(4-chlorobenzyl)-7-(difluoromethoxy)-1,2,3,4-tetrahydronaphthalen-2-yl]carbamate (30 mg, 0.069 mmol) was dissolved in dichloromethane (2 mL). 5N isopropanolic hydrochloric acid (0.3 mL) were added and the reaction mixture was stirred at room temperature for 3 h. The solvents were evaporated in vacuo. Yield: 26 mg (0.069 mmol, 100%, colorless solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096619B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d512dc53098a4f0fabc39a3a8506e312 |
| Source note | uspto-grants-2015_08 |