HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 57467309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 68513876 | HCID 68513876 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57467309 | HCID 57467309 | — |
Reaction Steps
N-{[7-Amino-8-benzyl-5,6,7,8-tetrahydronaphthalen-2-yl]methyl}propane-1-sulfonamide (cf. example 42) was acetylated in dichloromethane with acetyl chloride in the presence of ethyldiisopropylamine at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096619B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-43be1533a09e406e9bbec9a8aadf56d8 |
| Source note | uspto-grants-2015_08 |