HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 7010368, compound → HCID 86670522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 7010368 | HCID 7010368 | — |
| Reactant | HCID 86670523 | HCID 86670523 | — |
| Product | HCID 86670522 | HCID 86670522 | 44% |
Reaction Steps
In analogy to Example 5, 150 mg (0.29 mmol) of (8S,11R,13S,14S,17S)-17-hydroxy-11-[4-((S)-1-hydroxyethyl)phenyl]-1 3-methyl-17-pentafluoroethyl-1,2,6,7,8,11,12,13,14,15,16,17-dodecahydrocyclopenta[a]phenanthren-3-one were converted using (S)-2-allyloxycarbonylaminopropanoic acid and, after workup and purification, 87 mg (44%) of the title compound were isolated as a colourless foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096639B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-6a63c457441d433a907d98d5304f9533 |
| Source note | uspto-grants-2015_08 |