HuagongsheHuagongshe Chemistry Print Report · For research reference only
Styrene → HCID 131733269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Styrene | HCID 7501 | — |
| Reactant | N,N-Dimethylmethacrylamide | HCID 81465 | — |
| Catalyst | Azobisisobutyronitrile | HCID 6547 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 131733269 | HCID 131733269 | 71.5% |
Reaction Steps
0.67 g of styrene (ST), 1.23 g of N,N-dimethylmethacrylamide (DMMAA), 10 mg of azobisisobutyronitrile, and 5 ml of toluene were mixed, and a polymerization reaction was performed under a nitrogen atmosphere at 60° C. for 6 hours. After cooling, purification was performed by reprecipitation using chloroform-ether. Thus, 1.0 g of an ST-DMMAA (35:65) random copolymer was obtained. The ST-DMMAA (35:65) random copolymer had a number average molecular weight (Mn) of 78000.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096736B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-e2d8db4b57c746188c045a2628cb51e2 |
| Source note | uspto-grants-2015_08 |