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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 511053Generated: November 1, 2026

Styrene → HCID 131733269, compound

https://huagongshe.com/reaction/511053

Reaction equation

Participants

RoleNameHCIDCharge
ReactantStyreneHCID 7501—
ReactantN,N-DimethylmethacrylamideHCID 81465—
CatalystAzobisisobutyronitrileHCID 6547—
SolventTolueneHCID 1140—
ProductHCID 131733269HCID 13173326971.5%

Reaction Steps

0.67 g of styrene (ST), 1.23 g of N,N-dimethylmethacrylamide (DMMAA), 10 mg of azobisisobutyronitrile, and 5 ml of toluene were mixed, and a polymerization reaction was performed under a nitrogen atmosphere at 60° C. for 6 hours. After cooling, purification was performed by reprecipitation using chloroform-ether. Thus, 1.0 g of an ST-DMMAA (35:65) random copolymer was obtained. The ST-DMMAA (35:65) random copolymer had a number average molecular weight (Mn) of 78000.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09096736B2
Source datasetuspto-grants-2015_08
ORD IDord-e2d8db4b57c746188c045a2628cb51e2
Source noteuspto-grants-2015_08