HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluoro-5-methoxy-4-nitrobenzonitrile → 2-Fluoro-3-methoxy-4-nitrobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluoro-5-methoxy-4-nitrobenzonitrile | HCID 57955540 | — |
| Reactant | 1-Bromo-2-fluoro-3-methoxy-4-nitrobenzene | HCID 57955589 | — |
| Product | 2-Fluoro-3-methoxy-4-nitrobenzonitrile | HCID 57955549 | — |
Reaction Steps
The title compound was prepared according to the procedure for 3-fluoro-5-methoxy-4-nitrobenzonitrile (Compound 146F) using 1-Bromo-2-fluoro-3-methoxy-4-nitrobenzene (Compound 147G). 1H NMR (CDCl3, 400 MHz): δ=4.15 (d, J=2.27 Hz, 3 H), 7.45 (dd, J=8.59, 5.56 Hz, 1 H), 7.64 (dd, J=8.59, 1.77 Hz, 1 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09096624B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-f97f397d14944f2f9174a8a88c461ca5 |
| Source note | uspto-grants-2015_08 |