Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 511823Generated: November 2, 2026

Hydrochloride methanol → HCID 67291349, compound

https://huagongshe.com/reaction/511823

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloride methanolHCID 21893726—
ReactantHCID 68450007HCID 68450007—
ProductHCID 67291349HCID 6729134949%

Reaction Steps

(R)-N-((R)-1-(5-(cyclopropylmethoxy)pyridin-2-yl)ethyl)-2-methylpropane-2-sulfinamide (3.2 g, 10.9 mmol) was dissolved in 10N HCl/MeOH (50 mL). The mixture was stirred at room temperature for 3 hours. The mixture was concentrated by N2-flow to give the white precipitate. The solid was collected by filtration and washed with diisopropyl ether to give 3.2 g (49% yield) of the title compound as a white solid:

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09101616B2
Source datasetuspto-grants-2015_08
ORD IDord-d18ce5af483e4cf0a0fa2e753328258e
Source noteuspto-grants-2015_08