HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → 4-Phenoxybutyltriphenylphosphonium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | (4-Bromobutoxy)benzene | HCID 70986 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-Phenoxybutyltriphenylphosphonium bromide | HCID 49782785 | — |
Reaction Steps
The title compound was synthesized as in 6.1 using 4-phenoxybutyl bromide (5.2) (22.0 g, 95.9 mmol) and triphenylphosphine (27.6 g, 105.5 mmol) in anhydrous benzene (50 mL), to give 6.1 (40.0 g, 85% yield). White solid, m p 185-186° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-79808b9e92ef467da55b03576fdf429a |
| Source note | uspto-grants-2015_08 |