HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium fluoride → HCID 25017344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium fluoride | HCID 25516 | — |
| Reactant | HCID 25017341 | HCID 25017341 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 25017344 | HCID 25017344 | 180.1% |
| Product | HCID 25017345 | HCID 25017345 | — |
Reaction Steps
7-(3-Benzyloxy-phenyl)-heptanesulfonyl fluoride (13.2) was prepared as in 13.1 using 12.2 (0.149 g, 0.39 mmol) and NH4F (0.029 g, 0.78 mmol) in dry acetone (10 mL). Purification by flash column chromatography on silica gel gave the title compound (0.128 g, 91% yield) as a viscous liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-58149ba1ad4a4d1ba09f1489c98e0f66 |
| Source note | uspto-grants-2015_08 |