HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium fluoride → HCID 25017344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium fluoride | HCID 25516 | — |
| Reactant | HCID 25017342 | HCID 25017342 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 25017344 | HCID 25017344 | 183.7% |
| Product | HCID 25017346 | HCID 25017346 | — |
Reaction Steps
7-(2-Benzyloxy-phenyl)-heptanesulfonyl fluoride (13.3) was prepared as in 13.1 using 12.3 (0.09 g, 0.236 mmol) and NH4F (0.018 g, 0.486 mmol) in dry acetone (10 mL). Purification by flash column chromatography gave the title compound (0.079 g, 92% yield) as a viscous liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-b50643676a654107b90e9e82d4428503 |
| Source note | uspto-grants-2015_08 |