HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium fluoride → HCID 25017344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium fluoride | HCID 25516 | — |
| Reactant | HCID 25017343 | HCID 25017343 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 25017344 | HCID 25017344 | 251.7% |
| Product | HCID 44128291 | HCID 44128291 | — |
Reaction Steps
5-(4-Benzyloxy-phenyl)-pentanesulfonyl fluoride (13.4) was synthesized as described in 13.1 using, 12.4 (0.3 g, 0.87 mmol) and NH4F (0.06 g, 1.64 mmol) in dry acetone (40 mL). Purification by flash column chromatography on silica gel gave the title compound (0.266 g, 91% yield) as a white solid (m p 66-68° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-d8f1fa2ddabc4fb5a187c2ff357a1adf |
| Source note | uspto-grants-2015_08 |