HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cerium(III) chloride → HCID 66931212, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cerium(III) chloride | HCID 24636 | — |
| Reactant | HCID 20213174 | HCID 20213174 | — |
| Reactant | HCID 66930888 | HCID 66930888 | — |
| Reactant | HCID 86636788 | HCID 86636788 | — |
| Product | HCID 66931212 | HCID 66931212 | 55% |
Reaction Steps
The synthesis was carried out analogous to the preparation of 64.1 using 62.2 (0.1 g, 0.32 mmol), cerium chloride (0.44 g, 1.6 mmol) and 63 (0.42 g, 1.6 mmol). Purification by flash column chromatography on silica gel gave pure 64.2 (0.077 mg, 55% yield) as a white solid (m p 98-100° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09102622B2 |
| Source dataset | uspto-grants-2015_08 |
| ORD ID | ord-47e74e02460c4b2e9a99dc8f6c6b793d |
| Source note | uspto-grants-2015_08 |