Triacetoxyperiodinane → HCID 25018605, compound

Participants

Reaction Steps

The synthesis was carried out analogous to the preparation of 65.1 using 64.2 (60 mg, 0.15 mmol) and Dess-Martin periodinane (0.127 g, 0.3 mmol) in wet CH2Cl2 (5 mL). Purification by flash column chromatography on silica gel gave pure compound 65.2 (47.5 mg, 80% yield) as a white solid (m p 118-120° C.).

Provenance & Evidence