HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tributylamine → 5-Butoxy-4-methyl-1,3-oxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tributylamine | HCID 7622 | — |
| Reactant | n-Butyl alpha-isocyanopropionate | HCID 11171108 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | 5-Butoxy-4-methyl-1,3-oxazole | HCID 9877440 | — |
Reaction Steps
A continuously operated dividing wall column (4.8 m×64 mm) packed with 3×3 mm V2A Raschig rings and a dividing wall of height 2.4 m having 60 theoretical plates was charged with a mixture of 13.1% by weight of n-butyl α-isocyanopropionate (R1 =n-butyl, R2=methyl), 32.2% by weight of monochlorobenzene and 50.1% by weight of tri-n-butylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06713630B2 |
| Source dataset | uspto-grants-2004_03 |
| ORD ID | ord-03fcb0d775cb4cc78bd97c5afc46059b |
| Source note | uspto-grants-2004_03 |