2-Methylbenzoic acid → HCID 86716253, compound

HRID 512220Notes

Reaction equation

HRID 512220 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([CH:18]([CH2:24][NH2:25])[CH2:19][CH2:20][N:21]([CH3:23])[CH3:22])=[CH:14][CH:13]=1>>[Cl:11][C:12]1[CH:13]=[CH:14][C:15]([CH:18]([CH2:19][CH2:20][N:21]([CH3:23])[CH3:22])[CH2:24][NH:25][C:4](=[O:6])[C:3]2[CH:7]=[CH:8][CH:9]=[CH:10][C:2]=2[CH3:1])=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 83732-Methylbenzoic acidHCID 82081088HCID 82081088, compound

Product 1

HCID 86716253HCID 86716253, compound

Procedure

From 2-methylbenzoic acid and 3-(4-chloro-phenyl)-N1,N1-dimethyl-butane-1,4-diamine. LCMS (MH+): m/z=345.1, tR (minutes, Method A)=0.8

Sources & evidence

ORD record
ord-6206305f2740401dba6b82d837bf011c
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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