2,3-Dimethylbenzoic acid → HCID 86716255, compound

HRID 512222Notes

Reaction equation

HRID 512222 reaction equation
[CH3:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:12][CH:13]([CH3:25])[CH2:14][CH:15]([C:18]1[CH:19]=[N:20][C:21]([CH3:24])=[CH:22][CH:23]=1)[CH2:16][NH2:17]>>[CH3:1][C:2]1[C:10]([CH3:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:17][CH2:16][CH:15]([C:18]1[CH:19]=[N:20][C:21]([CH3:24])=[CH:22][CH:23]=1)[CH2:14][CH:13]([CH3:25])[CH3:12])=[O:6]

Participants

3

Reactant 2

HCID 117822,3-Dimethylbenzoic acidHCID 83818231HCID 83818231, compound

Product 1

HCID 86716255HCID 86716255, compound

Procedure

From 2,3-dimethylbenzoic acid and 4-methyl-2-(6-methylpyridin-3-yl)-pentylamine. LCMS (MH+): m/z=325.0, tR (minutes, Method A)=1.38

Sources & evidence

ORD record
ord-1e9a09f8da704412b5107d7c5bffe464
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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