2-Methylbenzoic acid → HCID 86716256, compound

HRID 512223Notes

Reaction equation

HRID 512223 reaction equation
[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:11][CH:12]([CH3:24])[CH2:13][CH:14]([C:17]1[CH:18]=[N:19][C:20]([CH3:23])=[CH:21][CH:22]=1)[CH2:15][NH2:16]>>[CH3:1][C:2]1[CH:10]=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:16][CH2:15][CH:14]([C:17]1[CH:18]=[N:19][C:20]([CH3:23])=[CH:21][CH:22]=1)[CH2:13][CH:12]([CH3:24])[CH3:11])=[O:6]

Participants

3

Reactant 2

HCID 83732-Methylbenzoic acidHCID 83818231HCID 83818231, compound

Product 1

HCID 86716256HCID 86716256, compound

Procedure

From 2-methylbenzoic acid and 4-methyl-2-(6-methylpyridin-3-yl)-pentylamine. LCMS (MH30 ): m/z=311.0, tR (minutes, Method A)=1.31

Sources & evidence

ORD record
ord-fbf2c4c5db03465eba2e4439ee36b250
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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