2,3-Dichlorobenzoic acid → HCID 86716293, compound

HRID 512254Notes

Reaction equation

HRID 512254 reaction equation
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH:12]1([CH2:15][CH:16]([C:19]2[CH:20]=[N:21][CH:22]=[C:23]([Cl:25])[CH:24]=2)[CH2:17][NH2:18])[CH2:14][CH2:13]1>>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:18][CH2:17][CH:16]([C:19]1[CH:20]=[N:21][CH:22]=[C:23]([Cl:25])[CH:24]=1)[CH2:15][CH:12]1[CH2:13][CH2:14]1)=[O:6]

Participants

3

Reactant 2

HCID 57652,3-Dichlorobenzoic acidHCID 86716294HCID 86716294, compound

Product 1

HCID 86716293HCID 86716293, compound

Procedure

From 2,3-dichlorobenzoic acid and 3-cyclopropyl-2-(5-chloro-pyridin-3-yl)-propylamine. LCMS (MH+): m/z=383.0, tR (minutes, Method D)=0.74

Sources & evidence

ORD record
ord-28532b5658f3403c8a452392ad95c718
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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