2,3-Dichlorobenzoic acid → HCID 86716395, compound

HRID 512343Notes

Reaction equation

HRID 512343 reaction equation
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:12][O:13][CH2:14][CH2:15][CH:16]([C:19]1[CH:20]=[N:21][C:22]([C:25]([F:28])([F:27])[F:26])=[N:23][CH:24]=1)[CH2:17][NH2:18]>>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:18][CH2:17][CH:16]([C:19]1[CH:20]=[N:21][C:22]([C:25]([F:28])([F:27])[F:26])=[N:23][CH:24]=1)[CH2:15][CH2:14][O:13][CH3:12])=[O:6]

Participants

3

Reactant 2

HCID 57652,3-Dichlorobenzoic acidHCID 86716396HCID 86716396, compound

Product 1

HCID 86716395HCID 86716395, compound

Procedure

From 2,3-dichlorobenzoic acid and 4-methoxy-2-(2-(trifluoromethyl)pyrimidin-5-yl)butan-1-amine. LCMS (MH+): m/z=422.0, tR (minutes, Method F)=2.73

Sources & evidence

ORD record
ord-0e6d0709aa184d18b64efb881288d4db
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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