2,4-Dichlorobenzoic Acid → HCID 86716421, compound

HRID 512367Notes

Reaction equation

HRID 512367 reaction equation
[Cl:1][C:2]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[C:12]1([CH:18]([C:21]2[CH:22]=[N:23][C:24]([C:27]([F:30])([F:29])[F:28])=[CH:25][CH:26]=2)[CH2:19][NH2:20])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[Cl:1][C:2]1[CH:10]=[C:9]([Cl:11])[CH:8]=[CH:7][C:3]=1[C:4]([NH:20][CH2:19][CH:18]([C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1)[C:21]1[CH:22]=[N:23][C:24]([C:27]([F:30])([F:28])[F:29])=[CH:25][CH:26]=1)=[O:6]

Participants

3

Reactant 2

HCID 57872,4-Dichlorobenzoic AcidHCID 86716422HCID 86716422, compound

Product 1

HCID 86716421HCID 86716421, compound

Procedure

From 2,4-dichlorobenzoic acid and 2-phenyl-2-(6-(trifluoromethyl)pyridin-3-yl)ethanamine. LCMS (MH+): m/z=439.0, tR (minutes, Method E)=0.81

Sources & evidence

ORD record
ord-08eb361a957c4053bf8a7c8605d27769
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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