2,3-Dichlorobenzoic acid → HCID 86716423, compound

HRID 512368Notes

Reaction equation

HRID 512368 reaction equation
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:12][C:13]1[N:18]=[CH:17][C:16]([C:19]2([CH2:24][NH2:25])[CH2:23][CH2:22][O:21][CH2:20]2)=[CH:15][N:14]=1>>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:25][CH2:24][C:19]1([C:16]2[CH:17]=[N:18][C:13]([CH3:12])=[N:14][CH:15]=2)[CH2:23][CH2:22][O:21][CH2:20]1)=[O:6]

Participants

3

Reactant 2

HCID 57652,3-Dichlorobenzoic acidHCID 83818313HCID 83818313, compound

Product 1

HCID 86716423HCID 86716423, compound

Procedure

From 2,3-dichlorobenzoic acid and (3-(2-methylpyrimidin-5-yl)tetrahydrofuran-3-yl)methanamine. LCMS (MH+): m/z=366.0, tR (minutes, Method E)=0.45

Sources & evidence

ORD record
ord-a3a3d17b813e4cdcac1fea8d6a7064a1
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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