2,3-Dichlorobenzoic acid → HCID 86716434, compound

HRID 512378Notes

Reaction equation

HRID 512378 reaction equation
[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:12][N:13]1[CH:17]=[C:16]([CH:18]([CH:21]2[CH2:26][CH2:25][O:24][CH2:23][CH2:22]2)[CH2:19][NH2:20])[CH:15]=[N:14]1>>[Cl:1][C:2]1[C:10]([Cl:11])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([NH:20][CH2:19][CH:18]([C:16]1[CH:15]=[N:14][N:13]([CH3:12])[CH:17]=1)[CH:21]1[CH2:22][CH2:23][O:24][CH2:25][CH2:26]1)=[O:6]

Participants

3

Reactant 2

HCID 57652,3-Dichlorobenzoic acidHCID 86716232HCID 86716232, compound

Product 1

HCID 86716434HCID 86716434, compound

Procedure

From 2,3-dichlorobenzoic acid and 2-(1-methyl-1H-pyrazol-4-yl)-2-(tetrahydro-2H-pyran-4-yl)ethanamine. LCMS (MH+): m/z=382.0, tR (minutes, Method E)=0.52

Sources & evidence

ORD record
ord-888920fb849a43c78d90a48fd8777d34
Source dataset
uspto-grants-2015_08
Patent number
US09102591B2

Reaction notes

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